HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl 3-phenyl-2-hydroxy-2-ethoxycarbonyl-propanoate → HCID 131720112, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl 3-phenyl-2-hydroxy-2-ethoxycarbonyl-propanoate | HCID 15828909 | — |
| Reactant | Lithium hydroxide methanol | HCID 23717829 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 131720112 | HCID 131720112 | — |
Reaction Steps
2 g of the ester are treated in MeOH with aqueous-methanol LiOH, as described above, to give 1.2 g of 3-phenyl-2-hydroxy-2-carboxy propanoic acid lithium salt, m.p. >300° C.:, I.R. 3400, 1640 cm-1 ; HNMR (D20) δ (TMS): 3,4 s, 7.2-7.35 m.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05656656 |
| Source dataset | uspto-grants-1997_08 |
| ORD ID | ord-d0ad9e3d69754a09ab60cd9e6cdfd5bb |
| Source note | uspto-grants-1997_08 |