HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 18915111, compound → HCID 18915181, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 18915111 | HCID 18915111 | — |
| Reactant | N,N-Dimethyl-3-morpholinemethanamine | HCID 18915134 | — |
| Solvent | Triethylamine | HCID 8471 | — |
| Product | HCID 18915181 | HCID 18915181 | 122.7% |
Reaction Steps
The procedure described in Example 24 was repeated, but using 0.90 g of 3-dimethylaminomethylmorpholine, 2.3 ml of triethylamine and 1.03 g of 5-chloro-3-oxoindan-1-carbonyl chloride, to afford 1.03 g of the title compound, melting at 230°-240° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05656758 |
| Source dataset | uspto-grants-1997_08 |
| ORD ID | ord-9758d50eaf13434cbed90838fb140ce4 |
| Source note | uspto-grants-1997_08 |