HuagongsheHuagongshe Chemistry Print Report · For research reference only
m-Chloroperbenzoic acid → 3-(N-Isopropyl-N-n-propylamino)-5-phenyl-1-oxothiochroman
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | m-Chloroperbenzoic acid | HCID 70297 | — |
| Reactant | 3-(N-Isopropyl-N-n-propylamino)-5-phenylthiochroman hydrochloride | HCID 19028087 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | 3-(N-Isopropyl-N-n-propylamino)-5-phenyl-1-oxothiochroman | HCID 19028148 | — |
Reaction Steps
3-(N-Isopropyl-N-n-propylamino)-5-phenylthiochroman hydrochloride (310 mg, 0.86 mmol) was dissolved in 6 mL chloroform and to the cooled solution (ice-bath) was m-chloroperbenzoic acid (348 mg, 1.72 mmol) added in one portion.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05656657 |
| Source dataset | uspto-grants-1997_08 |
| ORD ID | ord-c3e443a0f56e42a79b9508d8273d3204 |
| Source note | uspto-grants-1997_08 |