Methylamine hydrochloride → HCID 57753790, compound

HRID 225756Notes

Reaction equation

[N:1]1([CH2:6][CH2:7][CH2:8][O:9][C:10]2[CH:19]=[CH:18][C:17]3[CH2:16][N:15]([C:20]4[CH:21]=[CH:22][C:23]([C:26](O)=[O:27])=[N:24][CH:25]=4)[CH2:14][CH2:13][C:12]=3[N:11]=2)[CH2:5][CH2:4][CH2:3][CH2:2]1.Cl.[CH3:30][NH2:31]>>[CH3:30][NH:31][C:26]([C:23]1[CH:22]=[CH:21][C:20]([N:15]2[CH2:14][CH2:13][C:12]3[N:11]=[C:10]([O:9][CH2:8][CH2:7][CH2:6][N:1]4[CH2:2][CH2:3][CH2:4][CH2:5]4)[CH:19]=[CH:18][C:17]=3[CH2:16]2)=[CH:25][N:24]=1)=[O:27]

Participants

Reactant 2

HCID 6364545Methylamine hydrochloride

HCID 57753785HCID 57753785, compound

Product 1

HCID 57753790HCID 57753790, compoundYield 35%

Procedure

The title compound was prepared from the product of example 62 and methylamine hydrochloride, using a similar method to that of example 64, as a yellow gum in 35% yield.

Sources & evidence

ORD record: ord-a310e5e416954087a7a92f5ce7ebdc4d
Source dataset: uspto-grants-2009_07
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US07557121B2

Reaction notes

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