HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Iodopropane → HCID 22923342, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Iodopropane | HCID 33643 | — |
| Reactant | 6-Chloro-3-[1-(6,7-dimethoxy-4-quinazolinyl)-4-piperidinyl]-1,2,3,4-tetrahydro-2,4-dioxoquinazoline | HCID 22923543 | — |
| Product | HCID 22923342 | HCID 22923342 | 63% |
Reaction Steps
The procedure similar to that described in Example 1 was repeated, except that 300 mg (0.64 mmol) of Compound h was used in place of Compound 24 and propyl iodide was used in place of methyl iodide. As a result, 200.9 mg (yield: 63%) of Compound 42 was obtained as white crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05658917 |
| Source dataset | uspto-grants-1997_08 |
| ORD ID | ord-32fb10725af44cdfbbb40b34361636bc |
| Source note | uspto-grants-1997_08 |