HuagongsheHuagongshe Chemistry Print Report · For research reference only
Iodoethane → HCID 22923495, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Iodoethane | HCID 6340 | — |
| Reactant | 3-(1-Ethoxycarbonyl-4-piperidinyl)-1,2,3,4-tetrahydro-6-methyl-2,4-dioxoquinazoline | HCID 21851246 | — |
| Product | HCID 22923495 | HCID 22923495 | 79% |
Reaction Steps
The procedure similar to that described in Example 1 was repeated, except that 1.0 g (3.02 mmol) of 3-(1-ethoxycarbonyl-4-piperidinyl)-1,2,3,4-tetrahydro-6-methyl-2,4-dioxoquinazoline (Compound f) was used in place of Compound 24 and ethyl iodide was used in place of methyl iodide, whereby 855.0 mg (yield: 79%) of Compound b was obtained as white crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05658917 |
| Source dataset | uspto-grants-1997_08 |
| ORD ID | ord-beadcb6e96724a9b8a5533c57db9ed3f |
| Source note | uspto-grants-1997_08 |