HCID 87596239, compound → HCID 87596683, compound

Participants

Reaction Steps

The title compound was prepared from the compound of Example 12 in a similar manner to the compound of Example 2 as a white lyophilised powder (82%). δH NMR (d6 DMSO), 8.71 (0.8H, J 9.2 Hz), 8.61 (0.2H, d, J 9.5 Hz), 8.05 (0.8H, d, J 8.2 Hz), 7.56 (3H, br m), 7.14 (2H, m), 6.71 (0.2H, d, J 6.9 Hz), 5.51 (0.2H, d, J 8.4 Hz), 4.60 (0.8H, m), 4.49 (0.2H, m), 4.20 (0.4H, m), 3.71 (1.6H, t, J 8.5 Hz), 3.21 (0.8H, m), 3.11 (2H, m), 2.99 (0.8H, dd, J 13.8 and 9.5 Hz), 2.82 (0.2H, dd, J 13.7 and 10.3 Hz) 1.44 (10H, br m); m/z (ES+, 70 eV) 549 (M+H)+.

Provenance & Evidence