2,8-Diacetylamino-1-tetralone → HCID 22449524, compound

HRID 2257848Notes

Reaction equation

HRID 2257848 reaction equation
C(C1CCC2C(=C(C(=O)C)C=CC=2[F:14])C1=O)(=O)C.[C:19]([NH:22][CH:23]1[CH2:32][CH2:31][C:30]2[C:25](=[C:26]([NH:33]C(=O)C)[CH:27]=[CH:28][CH:29]=2)[C:24]1=[O:37])(=[O:21])[CH3:20]>>[C:19]([NH:22][CH:23]1[CH2:32][CH2:31][C:30]2[C:25](=[C:26]([NH2:33])[CH:27]=[CH:28][C:29]=2[F:14])[C:24]1=[O:37])(=[O:21])[CH3:20]

Participants

3

Reactant 2

HCID 120472982,8-Diacetylamino-1-tetraloneHCID 22449435HCID 22449435, compound

Product 1

HCID 22449524HCID 22449524, compound

Procedure

The reaction was carried out in the same manner as in Example 1-(4), except that 300 mg of the compound prepared in (1) above was used instead of 2,8-diacetylamino-1-tetralone of Example 1-(4), and post-treated to produce 182 mg of the title compound.

Workup

  1. additionpost-treated

Sources & evidence

ORD record
ord-7ed2aad50b2846028bf3cc02f7f30e96
Source dataset
uspto-grants-1997_08
Patent number
US05658920

Reaction notes

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