2,8-Diacetylamino-1-tetralone → HCID 22449505, compound

HRID 2257854Notes

Reaction equation

HRID 2257854 reaction equation
C([NH:4][C:5]1[CH:14]=[CH:13][C:12]([CH3:15])=[C:11]2[C:6]=1[C:7](=[O:16])[CH2:8][CH2:9][NH:10]2)(=O)C.[C:17]([NH:20]C1CCC2C(=C(NC(=O)C)C=CC=2)C1=O)(=O)[CH3:18]>>[NH2:4][C:5]1[CH:14]=[CH:13][C:12]([CH3:15])=[C:11]2[C:6]=1[C:7](=[O:16])[CH2:8][CH2:9][N:10]2[CH2:18][CH2:17][NH2:20]

Participants

3

Reactant 2

HCID 120472982,8-Diacetylamino-1-tetraloneHCID 22449436HCID 22449436, compound

Product 1

HCID 22449505HCID 22449505, compound

Procedure

The reaction was carried out in the same manner as in Example 1-(4), except that 510 mg of the compound prepared in (1) above was used instead of 2,8-diacetylamino-1-tetralone of Example 1-(4), and post-treated to produce 220 mg of the title compound.

Workup

  1. additionpost-treated

Sources & evidence

ORD record
ord-8a3e0c4a44da49968bf81b20aa0ab47d
Source dataset
uspto-grants-1997_08
Patent number
US05658920

Reaction notes

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