HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-(8-Oxo-5,6,7,8-tetrahydronaphthalen-1-YL)acetamide → 1-Acetyl-3,5-diacetylamino-8-chloro-2,3-dihydro-quinoline-4-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-(8-Oxo-5,6,7,8-tetrahydronaphthalen-1-YL)acetamide | HCID 12119265 | — |
| Reactant | 1-Acetyl-5-acetylamino-8-chloro-2,3-dihydroquinoline-4-one | HCID 22449421 | — |
| Product | 1-Acetyl-3,5-diacetylamino-8-chloro-2,3-dihydro-quinoline-4-one | HCID 22449510 | — |
Reaction Steps
The reaction was carried out in the same manner as in Example 1-(2), except that 1.4 gm of the compound prepared in (1) above was used instead of 8-acetylamino-1-tetralone of Example 1-(2). The reaction mixture obtained by the post-treatment was further reacted in the same manner as in Example 1-(3) and post-treated to produce 0.62 gm of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05658920 |
| Source dataset | uspto-grants-1997_08 |
| ORD ID | ord-3ab6b4effac847b191567138211419e9 |
| Source note | uspto-grants-1997_08 |