HCID 22923983, compound → HCID 178490108, compound

HRID 2257962Notes

Reaction equation

HRID 2257962 reaction equation
[CH3:1][O:2][C:3]1[CH:4]=[C:5]([CH2:9][CH2:10][C:11]([C:13]2[N:14]=[CH:15][N:16](C(C3C=CC=CC=3)(C3C=CC=CC=3)C3C=CC=CC=3)[CH:17]=2)=[O:12])[CH:6]=[CH:7][CH:8]=1.COC1C=C(C(C)C(C2N=CNC=2)=O)C=CC=1>>[CH3:1][O:2][C:3]1[CH:4]=[C:5]([CH2:9][CH2:10][C:11]([C:13]2[N:14]=[CH:15][NH:16][CH:17]=2)=[O:12])[CH:6]=[CH:7][CH:8]=1

Participants

3

Reactant 2

HCID 22923983HCID 22923983, compoundHCID 178490107HCID 178490107, compound

Product 1

HCID 178490108HCID 178490108, compound

Procedure

Using the same procedure as in Example 2.4.a and starting with 10.28 g (0.0217 mole) of 3-(3-methoxyphenyl)-1-(1-triphenylmethyl-1H-imidazol-4-yl)-1-propanone prepared in Example 2.3.b, 3.68 g of 3-(3-methoxyphenyl-1-(1H-imidazol-4-yl)-1-propanone are obtained after crystallization from ethyl acetate.

Workup

  1. customare obtained
  2. customafter crystallization from ethyl acetate

Sources & evidence

ORD record
ord-49aa2bce872b47429a8746f3fe926a5c
Source dataset
uspto-grants-1997_08
Patent number
US05658938

Reaction notes

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