HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → {3-[4-(aminoiminomethyl)benzyl]-2,5-dioxopyrrolidin-1-yl}acetyl-D,L-homophenylalanine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | {3-[4-(Aminoiminomethyl)benzyl]-2,5-dioxopyrrolidin-1-yl}acetyl-D,L-homophenylalanine methyl ester | HCID 131720120 | — |
| Product | {3-[4-(aminoiminomethyl)benzyl]-2,5-dioxopyrrolidin-1-yl}acetyl-D,L-homophenylalanine | HCID 131720121 | 55% |
Reaction Steps
45 mg of {3-[4-(aminoiminomethyl)benzyl]-2,5-dioxopyrrolidin-1-yl}acetyl-D,L-homophenylalanine methyl ester are allowed to stand at room temperature for 1 h with 5 ml of concentrated hydrochloric acid. The mixture is then concentrated to dryness in vacuo, and the residue is taken up in a little water and freeze-dried. 24 mg of {3-[4-(aminoiminomethyl)benzyl]-2,5-dioxopyrrolidin-1-yl}acetyl-D,L-homophenylalanine are obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05658935 |
| Source dataset | uspto-grants-1997_08 |
| ORD ID | ord-84d2c53eb5184f3bbb78ce998b973d01 |
| Source note | uspto-grants-1997_08 |