HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Heptanamine → HCID 22924144, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Heptanamine | HCID 8127 | — |
| Reactant | Ethyl 2-(4-formylphenoxy)-2-methylpropanoate | HCID 13134808 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 22924144 | HCID 22924144 | 92.6% |
Reaction Steps
The product from step (a) (4.72 g) was dissolved in absolute ethanol (140 ml) and n-heptylamine (2.3 g, Aldrich) added. The resulting solution was refluxed for one hour, 10% Pd/C added and the suspension placed on a Paar hydrogenation apparatus--uptake of hydrogen ceased after approximately ten minutes. The suspension was filtered and the filtrate evaporated in vacuo to give the desired product as a clear oil (6.2 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05658944 |
| Source dataset | uspto-grants-1997_08 |
| ORD ID | ord-b47d8b26e68f446184322f043665dad8 |
| Source note | uspto-grants-1997_08 |