HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 22902188, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Sulfuric Acid | HCID 1118 | — |
| Reactant | HCID 22924386 | HCID 22924386 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 22902188 | HCID 22902188 | 69.8% |
Reaction Steps
2 g of the product of Example C are refluxed for 2 hours in a mixture of 15ml of glacial acetic acid, 1.5 ml of water and 0.7 ml of concentrated sulphuric acid. The product is filtered off with suction at room temperature, washed with water and dried. 1.3 g of the title compound are obtained (71% of theory).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05659038 |
| Source dataset | uspto-grants-1997_08 |
| ORD ID | ord-7bc4c32a89aa474f8ef95ef16ed191b1 |
| Source note | uspto-grants-1997_08 |