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HRID22582

反应详情

EQUATION

反应方程式

HRID 22582 的结构方程式

REACTANTS

反应物

2
结构：Cc1ccc2ccc(Cl)cc2n1
HCID138395

7-Chloro-2-methylquinoline

C10H8ClN

结构：COC(=O)CCSC(SCCC(=O)OC)c1cccc(C=O)c1
HCID10021188

Dimethyl 3,3'-(((3-formylphenyl)methylene)bis(sulfanediyl))dipropanoate

C16H20O5S2

PRODUCTS

生成物

1
结构：COC(=O)CCSC(SCCC(=O)OC)c1cccc(C=Cc2ccc3ccc(Cl)cc3n2)c1
HCID53731421

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CC(=O)OC(C)=O
溶剂HCID7918

Acetic anhydride

C4H6O3

PROCEDURE

实验过程

A solution of aldehyde (Step 1) (5.2 g) and 7-chloroquinaldine were heated in 45 ml acetic anhydride for 48 hours. The reaction mixture was evaporated. Flash chromatography of the residue using 5% ethylacetate in hexane afforded the title compound.

WORKUP

后处理

  1. customThe reaction mixture was evaporated