4-Hexyloxyaniline → HCID 22923871, compound

HRID 2258312Notes

Reaction equation

HRID 2258312 reaction equation
[C:1]([C:4]1[CH:5]=[C:6]([O:14][CH3:15])[C:7]([C:10]([O:12][CH3:13])=[O:11])=[N:8][CH:9]=1)([OH:3])=O.[CH2:16]([O:22][C:23]1[CH:29]=[CH:28][C:26]([NH2:27])=[CH:25][CH:24]=1)[CH2:17][CH2:18][CH2:19][CH2:20][CH3:21]>C(OCC)C>[CH2:16]([O:22][C:23]1[CH:29]=[CH:28][C:26]([NH:27][C:1]([C:4]2[CH:5]=[C:6]([O:14][CH3:15])[C:7]([C:10]([O:12][CH3:13])=[O:11])=[N:8][CH:9]=2)=[O:3])=[CH:25][CH:24]=1)[CH2:17][CH2:18][CH2:19][CH2:20][CH3:21]

Participants

4

Reactant 2

HCID 383604-HexyloxyanilineHCID 22923859Methyl 5-carboxy-3-methoxypyridine-2-carboxylate

Product 1

HCID 22923871HCID 22923871, compound

Reagents, catalysts & solvents 1

HCID 3283Diethyl EtherSolvent

Procedure

Methyl 5-(((4-n-hexyloxyphenyl)amino)carbonyl)-3-methoxypyridine-2-carboxylate was prepared from methyl 5-carboxy-3-methoxypyridine-2-carboxylate and 4-hexyloxyaniline, m.p. 118°-119° C. (from diethyl ether).

Sources & evidence

ORD record
ord-68300b866cc3488c8a75a774322b4be1
Source dataset
uspto-grants-1997_08
Patent number
US05658933

Reaction notes

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