Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Dimethylformamide | HCID 6228 | — |
| Reactant | Indoline | HCID 10328 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 1-Bromoheptane | HCID 12369 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 53741928 | HCID 53741928 | — |
Reaction Steps
A mixture of indoline (17 parts), 1-bromoheptane (31 parts), potassium carbonate (24 parts) and N,N-dimethylformamide (30 parts) was stirred at 100° C. for 3 days. The cooled mixture was diluted with toluene, washed with water (×4), dried (MgSO4) and evaporated to leave 1-heptyl-2,3-dihydro-1H-indole (30 parts).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US05660598 |
|---|
| Source dataset | uspto-grants-1997_08 |
|---|
| ORD ID | ord-ddd07e0a333c4fc9bef68f3c5879ac25 |
|---|
| Source note | uspto-grants-1997_08 |
|---|
