HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2258380Generated: October 26, 2026
Dimethylformamide → N-butyl-N-(2-methylprop-2-eneyl)aniline
https://huagongshe.com/reaction/2258380
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Dimethylformamide | HCID 6228 | — |
| Reactant | 3-Chloro-2-methyl-1-propene | HCID 11241 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | N-Butylaniline | HCID 14310 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | N-butyl-N-(2-methylprop-2-eneyl)aniline | HCID 54010992 | — |
Reaction Steps
A mixture of N-butylaniline (12.35 parts), anhydrous potassium carbonate (17.1 parts), 3-chloro-2-methylpropene (11.24 parts) and DMF (20 parts) was stirred at 90° C. for 8 hours. The cooled mixture was poured into toluene, washed with water (×2), 1N hydrochloric acid (30 parts) and water (×2). The dried organic phase was evaporated to leave N-butyl-N-(2-methylprop-2-eneyl)aniline (14.3 parts).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US05660598 |
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| Source dataset | uspto-grants-1997_08 |
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| ORD ID | ord-fbce872db8c94b7daf813f5029f98905 |
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| Source note | uspto-grants-1997_08 |
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