HuagongsheHuagongshe Chemistry Print Report · For research reference only
O-Xylene → 1-Butyl-2,2-dimethylindoline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | O-Xylene | HCID 7237 | — |
| Reactant | N-butyl-N-(2-methylprop-2-eneyl)aniline | HCID 54010992 | — |
| Catalyst | Zincchloride | HCID 3007855 | — |
| Product | 1-Butyl-2,2-dimethylindoline | HCID 18788042 | — |
Reaction Steps
A mixture of N-butyl-N-(2-methylprop-2-eneyl)aniline (9.6 parts), zinc chloride (6.12 parts) and xylene (20 parts) was heated under reflux with vigorous stirring for 4.75 hours. The cooled mixture was filtered and the organic phase evaporated to leave 1-butyl-2,2-dimethylindoline (5.3 parts).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05660598 |
| Source dataset | uspto-grants-1997_08 |
| ORD ID | ord-7f603290ea884b37aa05920e12f26970 |
| Source note | uspto-grants-1997_08 |