HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Diethylenetriamine → 3-[6-[[[2-[(2-Aminoethyl)amino]ethyl]amino]acetyl amino]-1-oxohexyl]amino-alpha-ethyl-2,4,6-triiodobenzenepropanoic acid
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Diethylenetriamine | HCID 8111 | — |
| Edukt | 3-[[6-[(Chloroacetyl)amino]-1-oxohexyl]amino]-alpha-ethyl-2,4,6-triiodobenzenepropanoic acid | HCID 22921401 | — |
| Produkt | 3-[6-[[[2-[(2-Aminoethyl)amino]ethyl]amino]acetyl amino]-1-oxohexyl]amino-alpha-ethyl-2,4,6-triiodobenzenepropanoic acid | HCID 22921396 | 48% |
Reaktionsschritte
According to the procedure described in Example 1, 123 g of diethylenetriamine (0.16 mol) are reacted with 121.7 g of compound (A) 3-[[6-[(chloroacetyl)amino]-1-oxohexyl]amino]-α-ethyl-2,4,6-triiodobenzene propanoic acid. 64 g of 3-[6-[[[2-[(2-aminoethyl)amino]ethyl]amino]acetyl amino]-1-oxohexyl]amino-α-ethyl-2,4,6-triiodobenzenepropanoic acid (0.077 mol) are obtained.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05660814 |
| Quelldatensatz | uspto-grants-1997_08 |
| ORD ID | ord-ea061e85110a46328f899d27dccab96f |
| Quellennotiz | uspto-grants-1997_08 |