HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 131719083, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 4-Pyridinemethanamine | HCID 77317 | — |
| Reactant | 8-chlorodibenz[b,f][1,4]oxazepin-10(11H)carbonyl chloride | HCID 14975983 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 131719083 | HCID 131719083 | — |
Reaction Steps
By the method described in Example 18, the title compound of Example 2 in CH2Cl2 with molecular sieves #5A and Et3N was reacted with 4-(aminomethyl)pyridine to generate the free base of the title product. This material was converted to the title compound by the method described in Example 40.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05661146 |
| Source dataset | uspto-grants-1997_08 |
| ORD ID | ord-fb35ed4cce134f35a9ef53d9d260e439 |
| Source note | uspto-grants-1997_08 |