HuagongsheHuagongshe Chemistry Print Report · For research reference only
7-Chloro-2-(2-hydroxymethylbenzofuran-5-yl)quinoline → 7-Chloro-2-(2-formylbenzofuran-5-yl)quinoline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 7-Chloro-2-(2-hydroxymethylbenzofuran-5-yl)quinoline | HCID 22922214 | — |
| Catalyst | HCID 178418406 | HCID 178418406 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | 7-Chloro-2-(2-formylbenzofuran-5-yl)quinoline | HCID 22922181 | 85,318.898% |
Reaction Steps
A mixture of 7-chloro-2-(2-hydroxymethylbenzofuran-5-yl)quinoline (767.9 mg) and manganese (IV) oxide (5.01 g) in chloroform (80 ml) was stirred for 5 hours at ambient temperature. The resulting mixture was filtered and the filtrate was concentrated in reduced pressure to give 7-chloro-2-(2-formylbenzofuran-5-yl)quinoline (650.9 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05661159 |
| Source dataset | uspto-grants-1997_08 |
| ORD ID | ord-e81146bbffc3486db859a04f95fdb2a1 |
| Source note | uspto-grants-1997_08 |