Cyclohexylamine → HCID 10634737, compound

HRID 2258533Notes

Reaction equation

HRID 2258533 reaction equation
Cl[C:2]1[CH:7]=[C:6]([Cl:8])[CH:5]=[CH:4][C:3]=1[N+:9]([O-:11])=[O:10].[CH:12]1([NH2:18])[CH2:17][CH2:16][CH2:15][CH2:14][CH2:13]1>C(OCCO)C>[Cl:8][C:6]1[CH:5]=[CH:4][C:3]([N+:9]([O-:11])=[O:10])=[C:2]([NH:18][CH:12]2[CH2:17][CH2:16][CH2:15][CH2:14][CH2:13]2)[CH:7]=1

Participants

4

Reactant 2

HCID 7965CyclohexylamineHCID 118992,4-Dichloronitrobenzene

Product 1

HCID 10634737HCID 10634737, compound

Reagents, catalysts & solvents 1

HCID 8076Glycol monoethyl etherSolvent

Procedure

A mixture consisting of 19.4 g of 2,4-dichloro-1-nitrobenzene, 40 g of cyclohexylamine and 100 ml of 2-ethoxyethanol is maintained at reflux for 12 hours.

Workup

  1. temperatureis maintained
  2. temperatureat reflux for 12 hours

Sources & evidence

ORD record
ord-ae864035a70c4a5b9b260e52cdc7e34a
Source dataset
uspto-grants-1997_08
Patent number
US05661169

Reaction notes

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