HuagongsheHuagongshe Chemistry Print Report · For research reference only
Urea → 6-Chloro-1-cyclohexyl-1H-benzimidazol-2-ol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Urea | HCID 1176 | — |
| Reactant | HCID 12930161 | HCID 12930161 | — |
| Solvent | 1,2,3,4-Tetramethylbenzene | HCID 10263 | — |
| Product | 6-Chloro-1-cyclohexyl-1H-benzimidazol-2-ol | HCID 3061790 | — |
Reaction Steps
A mixture of 4.5 g of the compound obtained in Step B), 2.5 g of urea and 10 ml of 1,2,3,4-tetramethylbenzene is heated to 170°-180° C. for 90 minutes.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05661169 |
| Source dataset | uspto-grants-1997_08 |
| ORD ID | ord-aa6bde9ec99247d4b200c81a2bc232ea |
| Source note | uspto-grants-1997_08 |