HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 67559431, compound → HCID 44319223, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 67559431 | HCID 67559431 | — |
| Reactant | 2-[1-(3,4,5-Trimethoxy-benzoyl)-3-(3,4-dichloro-phenyl)-pyrrolidin-3-yl]-ethyl-methanesulfonate | HCID 86750906 | — |
| Product | HCID 44319223 | HCID 44319223 | — |
Reaction Steps
Prepare by the method of example 27.3.1 using 2-[3-(3,4-dichloro-phenyl)-1-(3,4,5-trimethoxy-benzoyl)-pyrrolidin-3-yl]-ethyl-methanesulfonate (0.75 g, 1.4 mmol) and 4-(3-methoxy-phenyl)-piperidine-4-carboxylic acid amide hydrochloride (0.5 g, 1.85 mmol) to give the title compound: Rf =0.43 (silica gel, 10% methanol/chloroform).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05661160 |
| Source dataset | uspto-grants-1997_08 |
| ORD ID | ord-a6cd4330e6794858a9d7b13641bbdf4d |
| Source note | uspto-grants-1997_08 |