HCID 17930140, compound → HCID 22593766, compound

HRID 225906Notes

Reaction equation

HRID 225906 reaction equation
[CH3:1][NH:2][C:3]([C:5]1[CH:14]=[CH:13][C:12]2[C:7](=[CH:8][CH:9]=[CH:10][CH:11]=2)[C:6]=1[CH3:15])=O.CNC(C1CC2C(C=1C)=CC=CC=2)=O>>[CH3:15][C:6]1[C:7]2[C:12](=[CH:11][CH:10]=[CH:9][CH:8]=2)[CH:13]=[CH:14][C:5]=1[CH2:3][NH:2][CH3:1]

Participants

3

Reactant 2

HCID 17930140HCID 17930140, compoundHCID 22593706HCID 22593706, compound

Product 1

HCID 22593766HCID 22593766, compoundYield 36%

Procedure

According to the procedure of Preparation 20(b), except substituting N,1-dimethylnaphthalene-2-carboxamide (0.3 g, 1.5 mmole) for the N,3-dimethylindene-2-carboxamide, the title compound (0.1 g, 36%) was prepared as a colorless oil: MS (ES) m/e 186 (M+H)+.

Sources & evidence

ORD record
ord-8f94ce7258dd4bfab15caabb4ba048e2
Source dataset
uspto-grants-2009_07
Patent number
US07557125B2

Reaction notes

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