Dodecanoyl chloride → HCID 53949329, compound

HRID 2259175Notes

Reaction equation

C([O:3][C:4](=[O:10])[C@H:5]([CH3:9])[NH:6][CH2:7][CH3:8])C.[C:11](Cl)(=[O:23])[CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH3:22]>>[CH2:7]([N:6]([C:11](=[O:23])[CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH3:22])[C@H:5]([C:4]([OH:10])=[O:3])[CH3:9])[CH3:8]

Participants

Reactant 2

HCID 8166Dodecanoyl chloride

HCID 22857660HCID 22857660, compound

Product 1

HCID 53949329HCID 53949329, compound

Procedure

Example 1A was repeated, replacing starting materials with N-ethyl alanine ethyl ester and dodecanoyl chloride and followed by hydrolysis to give N-Ethyl-N-(1-oxododecyl)alanine.

Workup

customfollowed by hydrolysis

Sources & evidence

ORD record: ord-96cdf8c7b98b4c0d90c1d7a1101f8a1f
Source dataset: uspto-grants-1995_12
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05472946

Reaction notes

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