Hydrochloric Acid → HCID 67803429, compound

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Reaction Steps

A 0.15 g sample of the compound from step 11a above was converted to the HCl salt by the procedure described in Example 1c. MS: 214 (M+H)+, 231 (M+NH4)+. NMR (D2O) δ: 1.89-2.35 (m, 4H), 3.43 (t, 2H, J=7.7 Hz), 4.10-4.18 (m, 1H), 4.27 (dd, 1H, J=8,10.7 Hz), 4.49 (dd, 1H, J=3, 10.7 Hz), 6.94-7.00 (m, 2H), 7.11-7.19 (m, 1H). Anal. Calcd for C11H14ClF2NO: C, 52.91; H, 5.65; N, 5.61; Found: C, 52.96; H, 5.42; N, 5.65.

Provenance & Evidence