Chlorine → HCID 19002778, compound

HRID 2259211Notes

Reaction equation

HRID 2259211 reaction equation
[CH3:1][O:2][C:3]1[CH:4]=[CH:5][C:6]2[CH:10]=[CH:9][S:8][C:7]=2[CH:11]=1.[Cl:12]Cl>>[CH3:1][O:2][C:3]1[CH:4]=[CH:5][C:6]2[CH:10]=[C:9]([Cl:12])[S:8][C:7]=2[CH:11]=1

Participants

3

Reactant 2

HCID 24526ChlorineHCID 136342376-Methoxy-1-benzothiophene

Product 1

HCID 19002778HCID 19002778, compound

Procedure

The same operations as in Preparation example 1 were carried out using 495 mg of 6-methoxybenzo[b]thiophene, and chlorine gas in place of cyclohexanone, and then purification was carried out by TLC (developing solvent, chloroform:n-hexane=4:1) to obtain 172 mg of 6-methoxy-2-chlorobenzo[b]thiophene.

Workup

  1. customThe same operations as in Preparation example 1
  2. custompurification

Sources & evidence

ORD record
ord-aaedd98cc0c34590ae04691b304f4679
Source dataset
uspto-grants-1995_12
Patent number
US05472962

Reaction notes

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