HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triphenylphosphine → HCID 88252522, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triphenylphosphine | HCID 11776 | — |
| Reactant | HCID 19002898 | HCID 19002898 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 88252522 | HCID 88252522 | 91% |
Reaction Steps
A solution of bromide (0.304 g, 1.16 mmol) of Step 2 and triphenylphosphine (0.455 g, 1.73 mmol) in 6 mL of acetonetrile was stirred at r.t. for 20 hr. Ether was added and the solid was washed with ether to yield 0.550 g (91%) of the title phosphonium salt.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05472964 |
| Source dataset | uspto-grants-1995_12 |
| ORD ID | ord-1d2b93d641694990af1b59c9a0c947d7 |
| Source note | uspto-grants-1995_12 |