Sodium Hydroxide → HCID 23685599, compound

HRID 2259747Notes

Reaction equation

HRID 2259747 reaction equation
[OH-].[Na+:2].[CH2:3]([C:6]1[C:7]([CH2:15][CH2:16][C:17]([OH:19])=[O:18])=[CH:8][C:9]2[O:13][CH2:12][O:11][C:10]=2[CH:14]=1)[CH2:4][CH3:5]>C(O)C>[CH2:3]([C:6]1[C:7]([CH2:15][CH2:16][C:17]([O-:19])=[O:18])=[CH:8][C:9]2[O:13][CH2:12][O:11][C:10]=2[CH:14]=1)[CH2:4][CH3:5].[Na+:2]

Participants

4

Reactant 2

HCID 14798Sodium HydroxideHCID 15819504HCID 15819504, compound

Product 1

HCID 23685599HCID 23685599, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

29.2 ml of a 1N aqueous sodium hydroxide solution and 100 ml of ethanol were added to 6.9 g of 3-(6-propyl-1,3-benzodioxole-5-yl)propionic acid to obtain a solution. The solvent was distilled off and ether was added to the residue. A precipitation thus formed was recovered by filtration and dried to obtain 7.5 g of the intended compound in the form of a colorless powder.

Workup

  1. customto obtain a solution
  2. distillationThe solvent was distilled off
  3. additionether was added to the residue
  4. customA precipitation
  5. customthus formed
  6. filtrationwas recovered by filtration
  7. customdried

Sources & evidence

ORD record
ord-4181e67f22ec4dc4b24e885087b6a96f
Source dataset
uspto-grants-1995_12
Patent number
US05475024

Reaction notes

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