2-Mercaptoethanol → HCID 19001647, compound

HRID 2259771Notes

Reaction equation

HRID 2259771 reaction equation
[O:1]1[C:5]2[CH:6]=[CH:7][C:8]([CH2:10][CH:11]([CH3:13])[SH:12])=[CH:9][C:4]=2[O:3][CH2:2]1.[SH:14][CH2:15][CH2:16][OH:17]>>[O:1]1[C:5]2[CH:6]=[CH:7][C:8]([CH2:10][CH:11]([S:12][S:14][CH2:15][CH2:16][OH:17])[CH3:13])=[CH:9][C:4]=2[O:3][CH2:2]1

Participants

3

Reactant 2

HCID 15672-MercaptoethanolHCID 19001657HCID 19001657, compound

Product 1

HCID 19001647HCID 19001647, compoundYield 64%

Procedure

5.0 g of the title compound was prepared from 8.4 g of 2-(1,3-benzodioxol-5-yl)-1-methylethanethiol and 2.24 g of 2-mercaptoethanol as a colorless oil according to the same procedure as that described in Example 1.

Sources & evidence

ORD record
ord-9b244e5865774da8811ee4b71145f2d7
Source dataset
uspto-grants-1995_12
Patent number
US05475024

Reaction notes

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