HuagongsheHuagongshe Chemistry Print Report · For research reference only
m-Tolyl isocyanate → HCID 9868877, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | m-Tolyl isocyanate | HCID 69303 | — |
| Reactant | HCID 22917832 | HCID 22917832 | — |
| Product | HCID 9868877 | HCID 9868877 | 53.3% |
Reaction Steps
Using a procedure similar to that described in Example 1, but starting with 2-[2-amino-N-(3-methoxyphenyl)acetamido]-N-methyl-N-phenylacetamide (1.6 g) and 3-methylphenyl isocyanate (0.67 g), and after recrystallisation in acetonitrile, 2-{N-(3-methoxyphenyl)-2-[3-(3-methylphenyl)ureido]acetamido}-N-methyl-N-phenylacetamide (1.2 g), m.p. 179° C., is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05475106 |
| Source dataset | uspto-grants-1995_12 |
| ORD ID | ord-df6d7ef8ba3441c1be275a2c5c00cd59 |
| Source note | uspto-grants-1995_12 |