HuagongsheHuagongshe Chemistry Print Report · For research reference only
m-Tolyl isocyanate → HCID 19002008, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | m-Tolyl isocyanate | HCID 69303 | — |
| Reactant | HCID 19001937 | HCID 19001937 | — |
| Product | HCID 19002008 | HCID 19002008 | 22.7% |
Reaction Steps
Using a procedure similar to that described in Example 1, but starting with tert-butyl 2-[2-amino-N-(3-trifluoromethylphenyl)acetamido]acetate (4.9 g) and 3-methylphenyl isocyanate (2 g), and after recrystallisation in diisopropyl ether, tert-butyl 2-{2-[3-(3-methylphenyl)ureido]-N-(3-trifluoromethylphenyl)acetamido}acetate (1.56 g), m.p. 140° C., is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05475106 |
| Source dataset | uspto-grants-1995_12 |
| ORD ID | ord-99e97292611d4c42a4889498c0041027 |
| Source note | uspto-grants-1995_12 |