HuagongsheHuagongshe Chemistry Print Report · For research reference only
m-Tolyl isocyanate → HCID 15670987, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | m-Tolyl isocyanate | HCID 69303 | — |
| Reactant | tert-butyl 2-{2-amino-N-[2-(N-methylanilino)carbonylphenyl]acetamido}acetate | HCID 19002033 | — |
| Product | HCID 15670987 | HCID 15670987 | 57.4% |
Reaction Steps
Using a procedure similar to that described in Example 27, but starting with tert-butyl 2-{2-amino-N-[2-(N-methylanilino)carbonylphenyl]acetamido}acetate (2.5 g) and 3-methylphenyl isocyanate (0.83 g), and after recrystallisation in ethyl acetate, tert-butyl 2-{N-[2-(N-methylanilino)carbonylphenyl]-2-[3-(3-methylphenyl)ureido]acetamido}acetate (1.9 g), m.p. 145° C., is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05475106 |
| Source dataset | uspto-grants-1995_12 |
| ORD ID | ord-ad0a3a16207d4f73bf6f6a061e9e58f5 |
| Source note | uspto-grants-1995_12 |