HuagongsheHuagongshe Chemistry Print Report · For research reference only
m-Tolyl isocyanate → HCID 19001989, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | m-Tolyl isocyanate | HCID 69303 | — |
| Reactant | HCID 19001930 | HCID 19001930 | — |
| Product | HCID 19001989 | HCID 19001989 | 26.3% |
Reaction Steps
Using a procedure similar to that described in Example 1, but starting with tert-butyl 2-[2-amino-N-(2-phenoxyphenyl)acetamido]acetate (4.7 g) and 3-methylphenyl isocyanate (1.9 g), and after recrystallisation in ethyl acetate, tert-butyl 2-{2-[3-(3-methylphenyl)ureido]-N-(2-phenoxyphenyl)acetamido}acetate (1.7 g), m.p. 204° C., is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05475106 |
| Source dataset | uspto-grants-1995_12 |
| ORD ID | ord-eea2a28fad324177aaf0ee31e6d5d079 |
| Source note | uspto-grants-1995_12 |