HCID 10579646, compound → HCID 54307072, compound

HRID 2260050Notes

Reaction equation

HRID 2260050 reaction equation
[CH3:1][C:2]1[N:3]=[C:4]2[C:9]([CH3:10])=[CH:8][N:7](CC3C=CC(C4C=CC=CC=4C4N(C(C5C=CC=CC=5)(C5C=CC=CC=5)C5C=CC=CC=5)N=NN=4)=CC=3)[N:5]2[N:6]=1.[CH3:48][C:49]1[N:50]([CH2:58][C:59]2[CH:64]=[CH:63][C:62]([C:65]3[CH:70]=[CH:69][CH:68]=[CH:67][C:66]=3[C:71]3[N:75]([C:76]([C:89]4[CH:94]=[CH:93][CH:92]=[CH:91][CH:90]=4)([C:83]4[CH:88]=[CH:87][CH:86]=[CH:85][CH:84]=4)[C:77]4[CH:82]=[CH:81][CH:80]=[CH:79][CH:78]=4)[N:74]=[N:73][N:72]=3)=[CH:61][CH:60]=2)[C:51]2[N:52]([N:54]=[CH:55][C:56]=2[CH3:57])[N:53]=1>>[CH3:48][C:49]1[N:50]([CH2:58][C:59]2[CH:60]=[CH:61][C:62]([C:65]3[CH:70]=[CH:69][CH:68]=[CH:67][C:66]=3[C:71]3[N:75]([C:76]([C:77]4[CH:82]=[CH:81][CH:80]=[CH:79][CH:78]=4)([C:89]4[CH:90]=[CH:91][CH:92]=[CH:93][CH:94]=4)[C:83]4[CH:88]=[CH:87][CH:86]=[CH:85][CH:84]=4)[N:74]=[N:73][N:72]=3)=[CH:63][CH:64]=2)[C:51]2[N:52]([N:54]=[CH:55][C:56]=2[CH3:57])[N:53]=1.[CH3:1][C:2]1[NH:3][C:4]2[N:5]([N:7]=[CH:8][C:9]=2[CH3:10])[N:6]=1

Participants

4

Reactant 2

HCID 10579646HCID 10579646, compound2×HCID 54307072HCID 54307072, compound

Product 2

HCID 54307072HCID 54307072, compoundHCID 178433780HCID 178433780, compound

Procedure

In the same manner as described in Example 38, 1.5 g of 2,7-dimethyl-5-[[2'-(N-triphenylmethyl-tetrazol-5-yl)biphenyl-4-yl]methyl]-5H-pyrazolo[1,5-b][1,2,4]triazole (compound 45a) and 560 mg of 2,7-dimethyl-1-[[2'-(N-triphenylmethyl-tetrazol-5-yl)biphenyl-4-yl]methyl]-1 H-pyrazolo[1,5-b][1,2,4]triazole (compound 45b) were obtained from 500 mg of 2,7-dimethyl-1H-pyrazolo[1,5-b][1,2,4]triazole.

Sources & evidence

ORD record
ord-aa47fab8646842cf91407c012623fed0
Source dataset
uspto-grants-1995_12
Patent number
US05475114

Reaction notes

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