HCID 10556259, compound → HCID 10556259, compound

HRID 2260051Notes

Reaction equation

HRID 2260051 reaction equation
[C:1]1([C:7]([C:82]2[CH:87]=[CH:86][CH:85]=[CH:84][CH:83]=2)([C:76]2[CH:81]=[CH:80][CH:79]=[CH:78][CH:77]=2)[N:8]2[C:12]([C:13]3[CH:18]=[CH:17][CH:16]=[CH:15][C:14]=3[C:19]3[CH:24]=[CH:23][C:22]([CH2:25][N:26]4[N:30]5[N:31]=[C:32]([CH2:34][CH2:35][CH3:36])[N:33]=[C:29]5[C:28](CC5C=CC(C6C=CC=CC=6C6N(C(C7C=CC=CC=7)(C7C=CC=CC=7)C7C=CC=CC=7)N=NN=6)=CC=5)=[C:27]4[CH2:74][CH3:75])=[CH:21][CH:20]=3)=[N:11][N:10]=[N:9]2)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[CH2:88]([C:90]1[CH:97]=[C:96]2[N:92]([N:93]=[C:94]([CH2:135][CH2:136][CH3:137])[N:95]2CC2C=CC(C3C=CC=CC=3C3N(C(C4C=CC=CC=4)(C4C=CC=CC=4)C4C=CC=CC=4)N=NN=3)=CC=2)[N:91]=1)[CH3:89].C(C1C(CC2C=CC(C3C=CC=CC=3C3N(C(C4C=CC=CC=4)(C4C=CC=CC=4)C4C=CC=CC=4)N=NN=3)=CC=2)=C2N(N=C(CCC)N2)N=1)C.C(C1N(CC2C=CC(C3C=CC=CC=3C3N(C(C4C=CC=CC=4)(C4C=CC=CC=4)C4C=CC=CC=4)N=NN=3)=CC=2)N2C(C=1)=NC(CCC)=N2)C>>[CH2:74]([C:27]1[N:26]([CH2:25][C:22]2[CH:21]=[CH:20][C:19]([C:14]3[CH:15]=[CH:16][CH:17]=[CH:18][C:13]=3[C:12]3[N:8]([C:7]([C:1]4[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=4)([C:82]4[CH:83]=[CH:84][CH:85]=[CH:86][CH:87]=4)[C:76]4[CH:77]=[CH:78][CH:79]=[CH:80][CH:81]=4)[N:9]=[N:10][N:11]=3)=[CH:24][CH:23]=2)[N:30]2[C:29]([CH:28]=1)=[N:33][C:32]([CH2:34][CH2:35][CH3:36])=[N:31]2)[CH3:75].[CH2:88]([C:90]1[CH:97]=[C:96]2[N:92]([N:93]=[C:94]([CH2:135][CH2:136][CH3:137])[NH:95]2)[N:91]=1)[CH3:89]

Participants

6

Reactant 4

HCID 10556259HCID 10556259, compoundHCID 19002221HCID 19002221, compound2×HCID 88419700HCID 88419700, compound2×HCID 178440297HCID 178440297, compound2×

Product 2

HCID 10556259HCID 10556259, compoundHCID 178440296HCID 178440296, compound

Procedure

In the same manner as described in Example 38, 0.49 g of 5,7-bis[[2'-(N-triphenylmethyl-tetrazol-5-yl)biphenyl-4-yl]methyl]-6-ethyl-2-propyl-5 H-pyrazolo[1,5-b][1,2,4]triazole (compound 47a), 2.30 g of 6-ethyl-2-propyl-1-[[2'-(N-triphenylmethyl-tetrazol-5-yl)biphenyl-4-yl]methyl]-1H-pyrazolo[1,5-b][1,2,4]triazole (compound 47b), 0.18 g of 6-ethyl-2-propyl-7-[[2'-(N-triphenylmethyl-tetrazol-5-yl)biphenyl-4-yl]methyl]-1H-pyrazolo[1,5-b][1,2,4]triazole (compound 47c) and 2.28 g of 6-ethyl-2-propyl-5-[[2'-(N-triphenylmethyl-tetrazol-5-yl)biphenyl-4-yl]methyl]-5H-pyrazolo[1,5-b][1,2,4]triazole (compound 47d) were obtained from 2.17 g of 6-ethyl-2-propyl-1H-pyrazolo[1,5-b][1,2,4]triazole.

Sources & evidence

ORD record
ord-1dc838a5b30749d8aee63dff66453a20
Source dataset
uspto-grants-1995_12
Patent number
US05475114

Reaction notes

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