HCID 10579985, compound → HCID 10579985, compound

HRID 2260052Notes

Reaction equation

HRID 2260052 reaction equation
[C:1]1([C:7]([C:81]2[CH:86]=[CH:85][CH:84]=[CH:83][CH:82]=2)([C:75]2[CH:80]=[CH:79][CH:78]=[CH:77][CH:76]=2)[N:8]2[C:12]([C:13]3[CH:18]=[CH:17][CH:16]=[CH:15][C:14]=3[C:19]3[CH:24]=[CH:23][C:22]([CH2:25][N:26]4[N:30]5[N:31]=[C:32]([CH2:34][CH3:35])[N:33]=[C:29]5[C:28](CC5C=CC(C6C=CC=CC=6C6N(C(C7C=CC=CC=7)(C7C=CC=CC=7)C7C=CC=CC=7)N=NN=6)=CC=5)=[C:27]4[CH2:73][CH3:74])=[CH:21][CH:20]=3)=[N:11][N:10]=[N:9]2)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[CH2:87]([C:89]1[N:90](CC2C=CC(C3C=CC=CC=3C3N(C(C4C=CC=CC=4)(C4C=CC=CC=4)C4C=CC=CC=4)N=NN=3)=CC=2)[C:91]2[N:92]([N:94]=[C:95]([CH2:97][CH3:98])[CH:96]=2)[N:93]=1)[CH3:88].C(C1NC2N(N=C(CC)C=2CC2C=CC(C3C=CC=CC=3C3N(C(C4C=CC=CC=4)(C4C=CC=CC=4)C4C=CC=CC=4)N=NN=3)=CC=2)N=1)C.C(C1N=C2C=C(CC)N(CC3C=CC(C4C=CC=CC=4C4N(C(C5C=CC=CC=5)(C5C=CC=CC=5)C5C=CC=CC=5)N=NN=4)=CC=3)N2N=1)C>>[CH2:34]([C:32]1[N:33]=[C:29]2[CH:28]=[C:27]([CH2:73][CH3:74])[N:26]([CH2:25][C:22]3[CH:21]=[CH:20][C:19]([C:14]4[CH:15]=[CH:16][CH:17]=[CH:18][C:13]=4[C:12]4[N:8]([C:7]([C:1]5[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=5)([C:81]5[CH:82]=[CH:83][CH:84]=[CH:85][CH:86]=5)[C:75]5[CH:76]=[CH:77][CH:78]=[CH:79][CH:80]=5)[N:9]=[N:10][N:11]=4)=[CH:24][CH:23]=3)[N:30]2[N:31]=1)[CH3:35].[CH2:87]([C:89]1[NH:90][C:91]2[N:92]([N:94]=[C:95]([CH2:97][CH3:98])[CH:96]=2)[N:93]=1)[CH3:88]

Participants

6

Reactant 4

HCID 10579985HCID 10579985, compoundHCID 10627907HCID 10627907, compound2×HCID 19002171HCID 19002171, compound2×HCID 178437910HCID 178437910, compound2×

Product 2

HCID 10579985HCID 10579985, compoundHCID 178435436HCID 178435436, compound

Procedure

In the same manner as described in Example 38, 0.31 g of 5,7-bis[[2'-(N-triphenylmethyl-tetrazol-5-yl)biphenyl-4-yl]methyl]-2,6-diethyl-5H-pyrazolo[1,5-b][1,2,4]triazole (compound 48a), 2.60 g of 2,6-diethyl-1-[[2'-(N-triphenylmethyl-tetrazol-5-yl)biphenyl-4-yl]methyl]-1H-pyrazolo[1,5-b][1,2,4]triazole (compound 48b), 0.20 g of 2,6-diethyl-7-[[2'-(N-triphenylmethyl-tetrazol-5-yl)biphenyl-4-yl]methyl]-1H-pyrazolo[1,5-b][1,2,4]triazole (compound 48c) and 2.04 g of 2,6-diethyl-5-[[2'-(N-triphenylmethyl-tetrazol-5-yl)biphenyl-4-yl]methyl]-5H-pyrazolo[1,5-b][1,2,4]triazole (compound 48d) were obtained from 2.00 g of 2,6-diethyl-1H-pyrazolo[1,5-b][1,2,4]triazole.

Sources & evidence

ORD record
ord-65b62c01d96849bcaa10e08534e69a2c
Source dataset
uspto-grants-1995_12
Patent number
US05475114

Reaction notes

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