HCID 10722447, compound → HCID 10722447, compound

HRID 2260055Notes

Reaction equation

HRID 2260055 reaction equation
[CH2:1]([C:3]1[N:4](CC2C=CC(C3C=CC=CC=3C3N(C(C4C=CC=CC=4)(C4C=CC=CC=4)C4C=CC=CC=4)N=NN=3)=CC=2)[C:5]2[N:6]([N:8]=[CH:9][CH:10]=2)[N:7]=1)[CH3:2].[CH2:48]([C:50]1[N:51]=[C:52]2[CH:57]=[CH:56][N:55]([CH2:58][C:59]3[CH:64]=[CH:63][C:62]([C:65]4[CH:70]=[CH:69][CH:68]=[CH:67][C:66]=4[C:71]4[N:75]([C:76]([C:89]5[CH:94]=[CH:93][CH:92]=[CH:91][CH:90]=5)([C:83]5[CH:88]=[CH:87][CH:86]=[CH:85][CH:84]=5)[C:77]5[CH:82]=[CH:81][CH:80]=[CH:79][CH:78]=5)[N:74]=[N:73][N:72]=4)=[CH:61][CH:60]=3)[N:53]2[N:54]=1)[CH3:49]>>[CH2:48]([C:50]1[N:51]=[C:52]2[CH:57]=[CH:56][N:55]([CH2:58][C:59]3[CH:60]=[CH:61][C:62]([C:65]4[CH:70]=[CH:69][CH:68]=[CH:67][C:66]=4[C:71]4[N:75]([C:76]([C:77]5[CH:82]=[CH:81][CH:80]=[CH:79][CH:78]=5)([C:89]5[CH:90]=[CH:91][CH:92]=[CH:93][CH:94]=5)[C:83]5[CH:88]=[CH:87][CH:86]=[CH:85][CH:84]=5)[N:74]=[N:73][N:72]=4)=[CH:63][CH:64]=3)[N:53]2[N:54]=1)[CH3:49].[CH2:1]([C:3]1[NH:4][C:5]2[N:6]([N:8]=[CH:9][CH:10]=2)[N:7]=1)[CH3:2]

Participants

4

Reactant 2

HCID 10722447HCID 10722447, compoundHCID 19002243HCID 19002243, compound2×

Product 2

HCID 10722447HCID 10722447, compoundHCID 178437908HCID 178437908, compound

Procedure

In the same manner as described in Example 38, 612 mg of 2-ethyl-1-[[2'-(N-triphenylmethyl-tetrazol-5-yl)biphenyl-4-yl]methyl]-1H-pyrazolo[1,5-b][1,2,4]triazole (compound 51a) and 449 mg of 2-ethyl-5-[[2'-(N-triphenylmethyl-tetrazol-5-yl)biphenyl-4-yl]methyl]-5H-pyrazolo[1,5-b][1,2,4]triazole (compound 51b) were obtained from 378 mg of 2-ethyl-1H-pyrazolo[1,5-b][1,2,4]triazole.

Sources & evidence

ORD record
ord-791f60b1059f4fa8b9a6635c07cdced4
Source dataset
uspto-grants-1995_12
Patent number
US05475114

Reaction notes

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