HCID 19002130, compound → HCID 19002130, compound

HRID 2260057Notes

Reaction equation

HRID 2260057 reaction equation
[CH3:1][C:2]1[N:3](CC2C=CC(C3C=CC=CC=3C3N(C(C4C=CC=CC=4)(C4C=CC=CC=4)C4C=CC=CC=4)N=NN=3)=CC=2)[C:4]2[N:5]([N:7]=[CH:8][CH:9]=2)[N:6]=1.[CH3:47][C:48]1[N:49]=[C:50]2[CH:55]=[CH:54][N:53]([CH2:56][C:57]3[CH:62]=[CH:61][C:60]([C:63]4[CH:68]=[CH:67][CH:66]=[CH:65][C:64]=4[C:69]4[N:73]([C:74]([C:87]5[CH:92]=[CH:91][CH:90]=[CH:89][CH:88]=5)([C:81]5[CH:86]=[CH:85][CH:84]=[CH:83][CH:82]=5)[C:75]5[CH:80]=[CH:79][CH:78]=[CH:77][CH:76]=5)[N:72]=[N:71][N:70]=4)=[CH:59][CH:58]=3)[N:51]2[N:52]=1>>[CH3:47][C:48]1[N:49]=[C:50]2[CH:55]=[CH:54][N:53]([CH2:56][C:57]3[CH:58]=[CH:59][C:60]([C:63]4[CH:68]=[CH:67][CH:66]=[CH:65][C:64]=4[C:69]4[N:73]([C:74]([C:81]5[CH:86]=[CH:85][CH:84]=[CH:83][CH:82]=5)([C:87]5[CH:88]=[CH:89][CH:90]=[CH:91][CH:92]=5)[C:75]5[CH:80]=[CH:79][CH:78]=[CH:77][CH:76]=5)[N:72]=[N:71][N:70]=4)=[CH:61][CH:62]=3)[N:51]2[N:52]=1.[CH3:1][C:2]1[NH:3][C:4]2[N:5]([N:7]=[CH:8][CH:9]=2)[N:6]=1

Participants

4

Reactant 2

HCID 19002130HCID 19002130, compoundHCID 19002197HCID 19002197, compound2×

Product 2

HCID 19002130HCID 19002130, compoundHCID 178433779HCID 178433779, compound

Procedure

In the same manner as described in Example 66, 2.61 g of 2-methyl-1-[[2'-(N-triphenylmethyl-tetrazol-5-yl)biphenyl-4-yl]methyl]-1H-pyrazolo[1,5-b][1,2,4]triazole (compound 72a) and 1.15 g of 2-methyl-5-[[2'-(N-triphenylmethyl-tetrazol-5-yl)biphenyl-4-yl]methyl]-5H-pyrazolo[1,5-b][1,2,4]triazole (compound 72b) were obtained from 1.11 g of 2-methyl-1H-pyrazolo[1,5-b][1,2,4]triazole.

Sources & evidence

ORD record
ord-77033a90e5e24403be5fc310832d0937
Source dataset
uspto-grants-1995_12
Patent number
US05475114

Reaction notes

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