HCID 19002208, compound → HCID 19002208, compound

HRID 2260058Notes

Reaction equation

HRID 2260058 reaction equation
[Cl:1][C:2]1[CH:3]=[N:4][N:5]2[C:9]=1[N:8](CC1C=CC(C3C=CC=CC=3C3N(C(C4C=CC=CC=4)(C4C=CC=CC=4)C4C=CC=CC=4)N=NN=3)=CC=1)[C:7]([CH2:47][CH3:48])=[N:6]2.[Cl:49][C:50]1[C:57]2[N:53]([N:54]=[C:55]([CH2:58][CH3:59])[N:56]=2)[N:52]([CH2:60][C:61]2[CH:66]=[CH:65][C:64]([C:67]3[CH:72]=[CH:71][CH:70]=[CH:69][C:68]=3[C:73]3[N:77]([C:78]([C:91]4[CH:96]=[CH:95][CH:94]=[CH:93][CH:92]=4)([C:85]4[CH:90]=[CH:89][CH:88]=[CH:87][CH:86]=4)[C:79]4[CH:84]=[CH:83][CH:82]=[CH:81][CH:80]=4)[N:76]=[N:75][N:74]=3)=[CH:63][CH:62]=2)[CH:51]=1>>[Cl:49][C:50]1[C:57]2[N:53]([N:54]=[C:55]([CH2:58][CH3:59])[N:56]=2)[N:52]([CH2:60][C:61]2[CH:62]=[CH:63][C:64]([C:67]3[CH:72]=[CH:71][CH:70]=[CH:69][C:68]=3[C:73]3[N:77]([C:78]([C:79]4[CH:84]=[CH:83][CH:82]=[CH:81][CH:80]=4)([C:91]4[CH:92]=[CH:93][CH:94]=[CH:95][CH:96]=4)[C:85]4[CH:90]=[CH:89][CH:88]=[CH:87][CH:86]=4)[N:76]=[N:75][N:74]=3)=[CH:65][CH:66]=2)[CH:51]=1.[Cl:1][C:2]1[CH:3]=[N:4][N:5]2[C:9]=1[NH:8][C:7]([CH2:47][CH3:48])=[N:6]2

Participants

4

Reactant 2

HCID 19002208HCID 19002208, compoundHCID 19002220HCID 19002220, compound2×

Product 2

HCID 19002208HCID 19002208, compoundHCID 178437911HCID 178437911, compound

Procedure

In the same manner as described in Example 66, 1.60 g of 7-chloro-2-ethyl-1-[[2'-(N-triphenylmethyl-tetrazol-5-yl)biphenyl-4-yl]methyl]-1H-pyrazolo[1,5-b][1,2,4]triazole (compound 73a) and 1.18 g of 7-chloro-2-ethyl-5-[[2'-(N-triphenylmethyl-tetrazol-5-yl)biphenyl-4-yl]methyl]-5H-pyrazolo[1,5-b][1,2,4]triazole (compound 73b) were obtained from 1.10 g of 7-chloro-2-ethyl-1H-pyrazolo[1,5-b][1,2,4]triazole.

Sources & evidence

ORD record
ord-7c76aa21e5ee4a88a9bfb70114126e5a
Source dataset
uspto-grants-1995_12
Patent number
US05475114

Reaction notes

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