反应详情

Octadecylamine (9.09 g, 0.034 mole) was dissolved in absolute ethanol. Glycidol (5.00 g, 0.068 mole) was added to the amine dropwise. The reaction solution was refluxed under nitrogen for 4 hours and then was stirred overnight at room temperature. A white solid was obtained (crude yield=10.8 g). The solid was recrystalized from hot hexane. (Yield=6.9 g).

1. temperatureThe reaction solution was refluxed under nitrogen for 4 hours
2. customA white solid was obtained (crude yield=10.8 g)
3. customThe solid was recrystalized from hot hexane