反应详情

N-(2,3-dihydroxypropyl)-N-dodecylamine (0.50 g, 0.0019 mole) and potassium hydroxide (0.01 g, 0.18 mmole) were heated to 85° C. under vacuum. Methyl palmitate (0.57 g, 0.0021 mole) was heated and added dropwise to the reaction. The reaction was heated under vacuum for 6 hours. A waxy off-white solid was obtained (crude yield=0.92 g) The waxy solid was recrystalized from hot hexane (yield=0.6 g).

1. additionadded dropwise to the reaction
2. temperatureThe reaction was heated under vacuum for 6 hours
3. customA waxy off-white solid was obtained (crude yield=0.92 g) The waxy solid
4. customwas recrystalized from hot hexane (yield=0.6 g)