反应详情

N-(2,3-dihydroxypropyl)-N-tetradecylamine (1.00 g, 0.0035 mole) and potassium hydroxide (0.01 g, 0.18 mmole) were heated to 85° C. under vacuum and methyl 2-hydroxyhexadecanoate (0.94 g, 0.0035 mole) was heated and added dropwise to the reaction. The reaction was heated under vacuum for 6 hours. A waxy off-white solid was obtained (crude yield=1.8 g). The waxy solid was recrystalized from hot hexane (yield=1.09 g)

1. temperaturewas heated
2. additionadded dropwise to the reaction
3. temperatureThe reaction was heated under vacuum for 6 hours
4. customA waxy off-white solid was obtained (crude yield=1.8 g)
5. customThe waxy solid was recrystalized from hot hexane (yield=1.09 g)