3,4-Dinitrobenzoic acid → 3,4-dinitrobenzoyl Chloride
Reaktionsgleichung
[N+:1]([C:4]1[CH:5]=[C:6]([CH:10]=[CH:11][C:12]=1[N+:13]([O-:15])=[O:14])[C:7](O)=[O:8])([O-:3])=[O:2].S(Cl)([Cl:18])=O>C1C=CC=CC=1.C1(C)C=CC=CC=1>[N+:1]([C:4]1[CH:5]=[C:6]([CH:10]=[CH:11][C:12]=1[N+:13]([O-:15])=[O:14])[C:7]([Cl:18])=[O:8])([O-:3])=[O:2]Komponenten
5
Edukt 2
Produkt 1
Reagenzien, Katalysatoren, Lösungsmittel 2
Versuchsvorschrift
Typically, the 3,4-dinitrobenzoic acid starting material is dissolved in an aprotic solvent such as benzene or toluene and refluxed with thionylchloride for a period of about 2-6 hours to form the desired 3,4-dinitrobenzoyl chloride.
Quellen und Nachweise
- ORD-Eintrag
- ord-d05fde9b74e8430eaa06ccbdb5e3666a
- Quelldatensatz
- uspto-grants-1995_12
- Patentnummer
- US05476849
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