HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,6-Diethylaniline → Dibenz(b,e)oxepin-11-carboxamide, 6,11-dihydro-N-(2,6-diethylphenyl)-2-methyl-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,6-Diethylaniline | HCID 11369 | — |
| Reactant | 6,11-Dihydro-2-methyldibenz[b,e]-oxepin-11-carboxylic acid | HCID 10106342 | — |
| Product | Dibenz(b,e)oxepin-11-carboxamide, 6,11-dihydro-N-(2,6-diethylphenyl)-2-methyl- | HCID 3072806 | 66.5% |
Reaction Steps
The similar procedures as in Example 1 were repeated except using 1.47 g of Compound A and 0.78 g of 2,6-diethylaniline in place of aniline to obtain 1.34 g of Compound 3.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05478835 |
| Source dataset | uspto-grants-1995_12 |
| ORD ID | ord-583b831b7fd2489b85a4f62c4542424f |
| Source note | uspto-grants-1995_12 |