HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Diisopropylaniline → Dibenz(b,e)oxepin-11-carboxamide, 6,11-dihydro-N-(2,6-bis(1-methylethyl)phenyl)-2-methyl-
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Diisopropylaniline | HCID 32484 | — |
| Edukt | 6,11-Dihydro-2-methyldibenz[b,e]-oxepin-11-carboxylic acid | HCID 10106342 | — |
| Produkt | Dibenz(b,e)oxepin-11-carboxamide, 6,11-dihydro-N-(2,6-bis(1-methylethyl)phenyl)-2-methyl- | HCID 3072807 | 94,8% |
Reaktionsschritte
The similar procedures as in Example 1 were repeated except using 1.20 g of Compound A and 1.00 g of 2,6-diisopropylaniline in place of aniline to obtain 1.85 g of Compound 4.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05478835 |
| Quelldatensatz | uspto-grants-1995_12 |
| ORD ID | ord-331cf4583d0546198a0894dcfb6724b2 |
| Quellennotiz | uspto-grants-1995_12 |