HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
2,4,6-Trimethylaniline → 2-Methyl-6,11-dihydro-dibenzo[b,e]oxepine-11-carboxylic acid (2,4,6-trimethyl-phenyl)-amide
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 2,4,6-Trimethylaniline | HCID 6913 | — |
| Edukt | 6,11-Dihydro-2-methyldibenz[b,e]-oxepin-11-carboxylic acid | HCID 10106342 | — |
| Produkt | 2-Methyl-6,11-dihydro-dibenzo[b,e]oxepine-11-carboxylic acid (2,4,6-trimethyl-phenyl)-amide | HCID 10429309 | 61,5% |
Reaktionsschritte
The similar procedures as in Example 1 were repeated except using 1.47 g of Compound A and 0.71 g of 2,4,6-trimethylaniline in place of aniline to obtain 1.20 g of Compound 9.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05478835 |
| Quelldatensatz | uspto-grants-1995_12 |
| ORD ID | ord-40dc5bf76d994de6b096fe3b1c1ee217 |
| Quellennotiz | uspto-grants-1995_12 |