化工社化工社 化学情報印刷レポート · 研究参考用
6,11-Dihydro-2-methyldibenz[b,e]-oxepin-11-carboxylic acid → 6,11-Dihydro-N-(2,6-diisopropyl-4-thiocyanatophenyl)-2-methyldibenz[b,e]oxepin-11-carboxamide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 6,11-Dihydro-2-methyldibenz[b,e]-oxepin-11-carboxylic acid | HCID 10106342 | — |
| 反応物 | 4-Amino-3,5-di(propan-2-yl)phenyl thiocyanate | HCID 18998488 | — |
| 生成物 | 6,11-Dihydro-N-(2,6-diisopropyl-4-thiocyanatophenyl)-2-methyldibenz[b,e]oxepin-11-carboxamide | HCID 18998484 | 78.6% |
反応手順
The similar procedures as in Example 1 were repeated except using 1.12 g of Compound A and 1.24 g of 2,6-diisopropyl-4-thiocyanatoaniline in place of aniline to obtain 1.63 g of Compound 31.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05478835 |
| 出典データセット | uspto-grants-1995_12 |
| ORD ID | ord-22e0d0af7369422387a48d9ec6e913a1 |
| 出典メモ | uspto-grants-1995_12 |